博馳智能液質(zhì)三重四極(TQ)質(zhì)譜產(chǎn)品包括用于樣品分析的液相色譜、三重四極桿質(zhì)譜儀。
將每一種分析方法優(yōu)化到實(shí)現(xiàn)分析物的色譜分離、高靈敏度檢測和分析。安益譜液質(zhì)聯(lián)用控制軟件幫助用戶節(jié)約樣品序列設(shè)置、提交、下發(fā)和運(yùn)行時間，使用戶能夠快速運(yùn)用。
LCMSMS TQ-9001產(chǎn)品特性
離子源
ESI/APCI快速切換、智能識別
即插即用、氣電自動對接安裝
90°直角噴霧、抗污染能力強(qiáng).
質(zhì)量分析器
串聯(lián)金屬四極桿設(shè)計(jì)，無限接近四極桿理論電場
前后預(yù)桿，有效平衡離子入射角度，消除邊緣場效應(yīng).
碰撞反應(yīng)池
180°碰撞反應(yīng)池，去除中性粒子干擾
具有軸線加速電場，減小MRM通道間串?dāng)_
組合陣列式碰撞氣體控制，保障碰撞反應(yīng)的高效進(jìn)行
強(qiáng)大的數(shù)據(jù)采集和分析軟件 —— B&C ITECH Chemstation
中(英)文操作界面
集成儀器控制、調(diào)諧校準(zhǔn)、數(shù)據(jù)采集、數(shù)據(jù)處理等功能
| 序號 | 名稱/型號/規(guī)格 | 數(shù)量 | 單位 | 備注 |
| 一 | 標(biāo)準(zhǔn)配置 | |||
| 1 | 主機(jī) | |||
| 1.1 | TQ-9001三重四極桿質(zhì)譜儀 | 1 | 臺 | 含ESI、APCI離子源，集成注射泵、切換閥，一體式差分渦輪分子泵400/300 L/s，前級機(jī)械泵40 m3/h |
| 1.2 | SPH1299 二元泵 | 1 | 臺 | 二元超高壓液相泵組，壓力1300 bar，內(nèi)置在線真空脫氣機(jī) |
| 1.3 | Alias 自動進(jìn)樣器 | 1 | 臺 | 制冷型、標(biāo)配2個48位樣品瓶架 |
| 1.4 | T190柱溫箱 | 1 | 臺 | |
| 1.5 | 溶劑柜 | 1 | 臺 | |
| 1.6 | 廢液底座 | 1 | 臺 | |
| 1.7 | SV40機(jī)械泵 | 1 | 臺 | 內(nèi)含預(yù)裝泵油1瓶 |
| 2.1 | B&C ITECH Chemstation V1.0數(shù)據(jù)采集軟件 | 1 | 套 | |
| 2.2 | B&C ITECH Chemstation數(shù)據(jù)處理軟件 | 1 | 套 | |
| 2.3 | ||||
| 3 | 外設(shè)/附件 | |||
| 3.1 | 啟動工具包： | 1 | 套 | 隨機(jī)工具盒1套； 軟件1個； 軟件U盤1個； ESI 調(diào)諧液1瓶； 注射泵連接套裝1套： 1ml 注射器、 魯爾接頭、PEEK管線、PEEK 接頭； 安裝搬運(yùn)工具1套； 真空連接套件： 波紋管1根，KF40 卡箍2個，KF40 中心支架2個 備用密封圈1套： 離子源密封圈4個 QJET前密封圈1個 QJET后密封圈1個 反吹氣密封圈1個； |
| 3.2 | 儀器說明書 | 1 | 份 | |
| 3.3 | 產(chǎn)品合格證、保修卡 | 1 | 套 | |
| 3.4 | ||||
| 選配品 | ||||
| 1.1 | 電腦 | 1 | 臺 | |
| 1.2 | 打印機(jī) | 1 | 臺 | |
| 2 | ||||
| 2.1 | UPS穩(wěn)壓電源 | 1 | 臺 | |
| 2.2 | 氮?dú)獍l(fā)生器 | 1 | 臺 | |
| 2.3 | ||||
| 4 | 備品/耗材 | |||
| 4.1 | 色譜柱 | 1 | 根 | |
| 4.2 | 樣品瓶 | 1 | 套 | |
| 4.3 | 樣品瓶蓋 | 1 | 套 | |
B&C ITECH TQ9001 Triple Quad LC-MS/MS System
Instrument Specifications
| Instrument Specification-Mass spectrometer (Triple Quadruple) | |
| Mass range(m/z) | 5-2000 amu |
| Scan speed | >10,000 amu/sec |
| Mass Resolution | Unit Resolution FWHM，0.6-0.8 amu |
| Mass stability | ± 0.1Da in 24 hours |
| Sensitivity MRM mode | ESI+, Reserpine 1 pg on column, MRM609/195，S/N > 200,000 |
| Repeatability | ESI+, Tacrolimus 5pg on column with 10 injections, Peak area RSD < 1.5%, Retention time RSD<0.25 |
| Scan types | Full scan MS and selected ion for both Q1 and Q3, product ion scan, precursor ion scan, neutral loss or gain scan, Multiple reaction monitoring (MRM) |
| Dynamic range | 6 orders of magnitude |
| Ionization source | Ion Source housing with ESI Probe or APCI probe (max temp: 750ºC) ESI flow rate range: 5 μL/min to 3 mL/min APCI flow rate range: 200 µL/min to 3 mL/min |
| Software | B&C ITECH Chemstation V1.0 |
| Instrument Specification-Liquid Chromatograph (UHPLC) | |
| Flow rate range | 0.001 - 2.00 ml/min, 0.001 ml/min increments |
| Pressure range | 0-1300 bar |
| Flow precision | ≤ 0.075 % RSD or 0.005 min SD, whichever is greater, H2O in a flow range of 0.200 - 2.000 mL/min |
| Flow accuracy | ± 1% or ± 10 μL/min, whichever is greater, H2O in a flow range of 0.200 - 2.000 mL/min |
| Gradient composition range | 0 - 99% (A in B) |
| Gradient composition accuracy | ± 0.5 % absolute from 5 - 95%, H2O in a flow range of 0.200 - 2.000 mL/min |
| Gradient composition precision | ≤ 0.15% or 0.01 min SD, whichever is greater, H2O in a flow range of 0.200 - 2.000 mL/min |
| Injection modes | Full loop, partial loopfill and µL pickup mode |
| Injection volume | Programmable from 0 uL-100 uL,1 µL increments |
| Reproducibility | RSD £ 0.3% for full loop injections |
| RSD £ 0.5% for partial loopfill injections, injection volumes > 5 µL at constant pressure RSD £ 1.0% for µL pickup injections, injection volumes > 5 µL | |
| Carry-over | < 0.05% with programmable needle wash |
| Viscosity range | 0.1 - 5 cP |
| Sample tray cooling | Built-in Peltier cooling Range: 4°C to Ambient - 3°C Temp: air temperature in sample compartment: 4°C ± 2°C (at temperature sensor) (Temperature at relative humidity of 80% and ambient temperature of 25°C) |
| Needle wash | Inside and outside needle wash with drying. Wash can be programmed between injections and between vials/wells. |
| Sample capacity | Microtiter plates: 2 Vials: 2x 48 (1.5 mL) – optional Microtiter plates according to SBS standards. 96-well high and low and 384-well. |
| Column Oven Temperature control mode | air circulation with heating module |
| Temperature range | ambient+5°C - 60°C, with 1°C increments |
| Temperature stability | Better than 0.1 °C |
| Column capacity | Maximum 2 column, Length150 mm |
